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|
 The
result of ppm level after purification
Solvent Type |
Expected Titration Results |
Alumina |
Sieves |
De-Gas |
Copper |
Acetonitrile |
15 ppm |
* |
|
+ |
|
Benzene |
4 ppm |
* |
|
+ |
# |
Chloroform |
2 ppm |
* |
|
+ |
|
Dichloromethane |
2 ppm |
* |
|
+ |
|
DME |
30 ppm |
* |
|
+ |
|
DMF |
30 ppm |
|
* |
+ |
|
Ether - Inhibitor-free |
8 ppm |
* |
|
+ |
|
Heptane |
2 ppm |
* |
|
+ |
# |
Hexane |
2 ppm |
* |
|
+ |
# |
Hexanes |
2 ppm |
* |
|
+ |
# |
Methanol |
40 ppm |
* |
|
+ |
|
Pentane |
2 ppm |
* |
|
+ |
# |
Chlorobenzene |
6 ppm |
* |
|
+ |
|
THF - Inhibitor-free |
7 ppm |
* |
|
+ |
|
Toluene |
2 ppm |
* |
|
+ |
# |
* = Solvent will be dried using identified material.
+ = All Solvents must be de-gassed for oxygen removal using inert gas. De-gas times are located in Manual.
# = Identified solvents may be passed through Copper Catalyst for optimum oxygen scrubbing.
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